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測硫儀常見問題及處理方法

发布时间：2010-04-10 点击次数：1848次

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☆關于電解液的配制：

稱取 5 克碘化鉀， 5 克溴化鉀，溶于 250 毫升蒸餾水中，然後加 10 毫升冰乙酸即可。電解液可重複使用，用的時間長短根據重複使用次數和試樣含硫量高低而定。電解液的 PH 值在 1-3 時，可以使用，但 PH 值小于 1 時，應重新配制電解液。

☆關于煤樣的制備:

在試樣稱量前，應盡可能的將試樣瓶內的試樣混和均勻，最好用手捏住帶蓋的試樣瓶上方，手腕自上而下的做圓周運動，切勿上下搖動試樣瓶。或打開瓶蓋用稱樣勺攪拌試樣。試樣充分混和是確保結果精確和准確的關鍵。

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