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KZDL-8A 快速智能定硫儀操作規程

发布时间：2011-03-15 点击次数：1596次

KZDL-8A 快速智能定硫仪操作规程

一、打開定硫儀主機電源，等待定硫儀升溫，升到設定溫度1050℃。
二、打開淨化器電源，關閉二通閥，將所配制的電解液吸入電解池中。
電解液配制方法：用燒杯量取250ml蒸餾水，稱取5g碘化鉀和5g溴化鉀倒入蒸餾水中，用10ml量筒量取10ml冰乙酸倒入蒸餾水中，攪拌均勻溶解完即可。
三、檢查氣密性，將兩通閥關閉，觀察流量計指示是否能降到最低，如果不能降到最低，則爲漏氣現象。應檢查電解池的密封圈、膠塞和淨化器上的三支幹燥管上的塞子是否塞緊不漏氣。
四、打開兩通閥，將流量計調到1.0ml。打開攪拌開關，將主機上的【電解開關】打開，開始做實驗。
将称好的煤样（50.0mg）放入石英舟中，在面板上按【启动】，输入所称的煤样重量（三位数，例500），再按【启动】即可，结果将自动打印。
注：每次开机或停止做样20分钟，应先做废样（和做煤样相同），打印结果含硫量不为零时，下一个就可以做煤样了。

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